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The environmental scanning electron microscope (ESEM) allows one to investigate wet samples. Here we can see a morphological changes on the crystals of the Sm (Cu)-CB [6] system after extreme process of hydration/dehydration in the ESEM.

Click on the link below to see the complete experiment:

youtu.be/dWnC4QRPLP8

  

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 600X

Horizontal Field Width: 497 µm

Voltage: 20 kV

Spot: 3.0

Detector: GSED

 

The image presents CoNi nonowires with mushrooms. It is a mix image of ETD and CBS detector, it was take at 5kV, spot 2.0. the nanowires were raised into a organic membrane.

 

Courtesy of Dr. Berbecaru Andrei , UPB-ECOMET

 

Image Details

Instrument used: Quanta SEM

Magnification: 30,000x

Horizontal Field Width: 13,8

Vacuum: High Vacum

Voltage: 5kV

Spot: 2.0

Working Distance: 9.9

Detector: SE+BSE

 

An image of a titanium oxide layer formed during high temperature oxidation

 

Courtesy of Mr. Radosław Swadźba

 

Image Details

Instrument used: Inspect

Magnification: 1000

Voltage: 15kV

Spot: 4

Working Distance: 8.3

Detector: BSE

 

polymethacrylate droplets

 

Courtesy of Mr. MUHAMMET AYDIN

 

Image Details

Instrument used: Quanta SEM

Magnification: 8000

Voltage: 2

Spot: 3.5

Working Distance: 7

Detector: lfd

 

Zinc crystals that have been adsorbed on the surface of an alginate gel after being subjected to a process of wastewater treatment.

An important field of application of the alginates gels is the protection of the environment: alginate gels are used as adsorbents for the removal of heavy metals such as cadmium, zinc, lead, chromium and mercury in wastewater.

 

Courtesy of Dr. Maria Carbajo

 

Image Details

Instrument used: Quanta SEM

Magnification: 3000x

Horizontal Field Width: 100 um

Vacuum: 1.21x10-3 Pa

Voltage: 15 kV

Spot: 5.0

Working Distance: 10 mm

Detector: SE

 

Silver nanoprotrusions grown from a nanocrystal film by applying an electric field near a metal pad, which elevates as a wall.

 

Courtesy of Dr. Davide Spirito , Istituto Italiano di Tecnologia

 

Image Details

Instrument used: Helios NanoLab

Magnification: 8000x

Horizontal Field Width: 18.7 um

Voltage: 5 kV

Working Distance: 4.2

 

This scanning electron microscopy image shows the tip of a hard disk drive (HDD) read/write device, the magnetoresistive (MR) head assembly. This is the component that floats over the rotating magnetic disk inside a HDD and reads/writes the information recorded on it.

 

The slider (white rectangular piece, centered on the image) is what actually floats or slides over the surface of the magnetic disk, carrying the head at the correct distance from the medium (magnetic disk) for reading/writing. The complex forms over the surface of the slider (black and grey colors) are designed to maintain the same floating height above the disk surface, whether the slider is positioned above the inner or outer cylinders of the disk (the inner or outer part of the rotating magnetic disk). The linear speed of the rotating magnetic disk is different depending on the radial position of the MR head over the disk, so the air pressure between the slider and the magnetic disk is compensated thanks to this special designs to maintain the same reading/writing distance between the two parts and not lose performance or functionality.

 

The read/write sensors are the small straight pink lines over the black surface of the slider, on the right side of it.

  

Courtesy of Mr. Marcos Rosado , Institut Catala de Nanociencia i Nanotecnologia

 

Image Details

Instrument used: Quanta SEM

Vacuum: High Vacuum

Voltage: 5 kV

Spot: 3.0

Working Distance: 22 mm

Detector: SE

 

Flakes of raw vermiculite concentrate are micaceous in appearance and contain interlayer water in their structure. When the flakes are heated rapidly at a temperature above 870° C, the water flashes into steam, and the flakes expand into accordion like particles. This process is called exfoliation, or expansion, and the resulting lightweight material is chemically inert, fire resistant, and odorless. In lightweight plaster and concrete, vermiculite provides good thermal insulation. Vermiculite can absorb such liquids as fertilizers, herbicides, and insecticides, which can then be transported as free-flowing solids.

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 172x

Horizontal Field Width: 1730 µm

Vacuum: 120 Pa

Voltage: 25 kV

Spot: 3.0

Working Distance: 20.6

Detector: MIX: SE plus BSE

 

The silicon nanopillars are fabricated through combining two techniques, a gold mask made by nanosphere lithography and a Metal-Assisted Chemical Etching of Silicon.

The structures shown in the imagen look like an amazing coral reef, but at the nanoscale

  

Courtesy of Marcos Rosado

 

Image Details

Instrument used: Magellan

Magnification: 13.000x

Horizontal Field Width: 23 um

Vacuum: 5 x 10E-5 Pa

Voltage: 2kV

Spot: 100 pA

Working Distance: 5.2

Detector: vCD

 

Porcine gelatin containing natural dye developed to increase the potential application of natural dyes in powder for preparation of desserts, drinks, jelly beans, confectionery, in order to make these healthier food products and reduce the consumption of artificial dyes directly related to toxicological problems to human health. The image shows the high power particles present to absorb moisture and become swollen.

 

Courtesy of Dr. Thaís Passos

 

Image Details

Instrument used: Quanta SEM

Magnification: 10.000x

Horizontal Field Width: 29,8 µm

Vacuum: 4.76e-3 Pa

Voltage: 20 kV

Spot: 2.0

Working Distance: 15.8 mm

Detector: Mix - BSE plus SE

 

Synthesis of noble metal nanoparticles by green technique .

 

Courtesy of Mr. Durga Prasad Muvva , UGC-Networking Resource Centre, School of Chemistry and The Centre for Nanotechnology, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 9.9k

Voltage: 200 kV

Spot: 1

Working Distance: 3

 

The image was taken on our XL30 SFEG in Back Scatter mode and is of a pocket of naturally formed Barium Sulphate crystals found in a piece of Botryoidal Hematite from Western Australia.

 

Courtesy of Mrs. Christine Kimpton , Cranfield University

 

Image Details

Instrument used: Other FEI SEM (XL SEM, Sirion, etc.)

Magnification: 1500X

Horizontal Field Width: 80microns

Voltage: 20kv

Spot: 4

Working Distance: 10mm

Detector: BSE

 

A molecular model of a new metal organic framework (MOF) which selectively traps xenon, a gas that is released during reprocessing of nuclear fuel.

 

Terms of Use: Our images are freely and publicly available for use with the credit line, "Courtesy of Pacific Northwest National Laboratory." Please use provided caption information for use in appropriate context.

Inside of a multilayers photovoltaic panel. The cross section was perfomed with FIB.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 12000x

Horizontal Field Width: 24.9 μm

Voltage: 15kV

Spot: 6.5

Working Distance: 13.0 mm

Detector: SE

 

Aberration-corrected TEM image of a cerium oxide (CeO2) nanocube - the nanoscale engineering of oxides to expose highly-reactive facets has been shown to enhance the exchange activity. Thus, it is desirable to design materials to maximize their functionality. Image was taken at a dose of 1000 e-/Angstrom^2 using a single electron detection camera (Gatan K2 IS).

 

Courtesy of Mr. Ethan Lawrence , Arizona State University

 

Image Details

Instrument used: Titan

Magnification: 410000

Vacuum: 1E-7 mbar

Voltage: 300kV

Spot: 3

Detector: Gatan K2 IS

 

This image corresponds to the process of manufacturing of a ceramic lamella by focused ion beam (FIB) for later viewing by transmission electron microscopy.

 

Specifically, we can observe the instant in which the lamella, attached to Omniprobe micromanipulator, approaches the grid.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 1300x

Vacuum: 5x10-4 Pa

Voltage: 30 kV

Detector: CDEM

 

PNNL scientists research materials that mimic the chemical and physical aspects of debris from nuclear explosions in the environment and discover signatures that can be used to prevent proliferation of nuclear weapons. Shown here is a sheet of copper exposed to a plasma flame (~8,300 degrees Celsius) for several seconds. The image was taken by scientists Alison Eckberg and Ben Garcia of material created by researcher Martin Liezers; Greg Eiden is project principal investigator.

 

Terms of Use: Our images are freely and publicly available for use with the credit line, "Courtesy of Pacific Northwest National Laboratory." Please use provided caption information for use in appropriate context.

Image of a Christmas tree milled into a 100 nm thick gold layer.

 

Courtesy of Dr. Thomas Loeber , TU Kaiserslautern NSC

 

Image Details

Instrument used: Helios NanoLab

Magnification: 5,000x

Horizontal Field Width: 41.1 µm

Voltage: 2 kV

Working Distance: 3.7 mm

Detector: SE

 

Cross-transverse view of a cigarette filter, showing cellulose acetate fibers.

Ingestion or inhalation of fragments of cigarette filter fibers is a health problem for almost all smokers, but also contributes to the formation of lung cancer.

Smoking is a trap. Quit now!

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 5000x

Horizontal Field Width: 59.7 µ

Vacuum: 110 Pa

Voltage: 20 kV

Spot: 3.0

Working Distance: 15.1

Detector: MIX: SE plus BSE

 

Preparation of a lamella by focused ion beam (FIB) milling, for later viewing with TEM.

The material is a semiconductor integrated circuit (IC) chip with micro-structure-surface passivation film

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 7000x

Horizontal Field Width: 45 μm

Voltage: 15kV

Spot: 5.5

Working Distance: 8.3mm

Detector: SE

 

Microparticles formed by nanostructured hydroxyapatite crystals and biopolymers. Hydroxiapatite (HA) is one of the most biocompatible ceramics because it is similar to the mineral constituents of human bone and teeth. This composite are interesting biomaterial for medical applications, especially for bone replacement. The colors were obtained using the software FEI Company

 

Courtesy of Mr. Izamir Resende

 

Image Details

Instrument used: Quanta SEM

Magnification: 50,000X

Horizontal Field Width: 5,97µm

Vacuum: 0,0000325 mbar

Voltage: 20 kV

Spot: 2.0

Working Distance: 9.0 mm

Detector: SE

 

Fly head

 

Courtesy of Dr. Jon Ajuria

 

Image Details

Instrument used: Quanta SEM

 

It's a contamination of iron oxide involving the tungsten filament of an automotive light bulb.

 

Courtesy of Mr. FRANCISCO RANGEL , MCT/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 3963x

Horizontal Field Width: 75.3 μm

Vacuum: 9.27e-7 mbar

Voltage: 20 kV

Spot: 2.0

Working Distance: 10.8

Detector: Mix: SE plus BSE.

 

The red velvet mite is an arachnid that belongs to the family Trombidiidae. In India it is used as medicine for paralysis.

The figure represents the leg-mechanosensory hairs of Red Velvet spider. Such hair helps in sensing chemicals of the surrounding.

The work involved for developing Artificial Sensor useful for human being .

The amazing similarity to a real grass inspired me to take an image for contest.

  

Courtesy of Mr. SHIV KUMAR VERMA , National Institute of Technology, Rourkela

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 5,000x

Horizontal Field Width: 10μm

Vacuum: 0.00003 mbar

Voltage: 10KV

Spot: 3.0

Working Distance: 3.4

Detector: SE

 

Detail of the interdigital structure of the micromechanical device based on polysilicon.

 

Courtesy of Dr. Alexey Kolomiytsev , Southern Federal University

 

Image Details

Instrument used: Other FEI DualBeam (Altura, Expida, etc.)

Magnification: 2,000x

Horizontal Field Width: 128 μm

Vacuum: 5e-5 Pa

Voltage: 10 kV

Spot: 4.0

Working Distance: 5.0

Detector: CDEM

 

Microstructure of a steel alloy widely used in the oil and gas industries.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 10,000x

Horizontal Field Width: 29.8 µm

Voltage: 20 kV

Spot: 5.0

Working Distance: 12.9

Detector: Mix: SE plus BSE.

 

A portrait of an ant we made as a demonstration for a group of high-school students to show how an SEM works. The ant was coated with gold prior to imaging.

 

Courtesy of Dr. Martin Jonsson-Niedziolka , Institute of Physical Chemistry, Polish Academy of Sciences

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 78

Voltage: 5 kV

Spot: 4.0

Working Distance: 4.8

Detector: ETD

 

A microscopical structure carved out of an aluminium alloy using an ion gun. In order to achieve a higher quality, a square-shaped area was first coated with platinum within the scanning electron microscope. In the next step the "face" was drawn within the program and the selected sites were milled away with the focused beam of Ga ions. The image was taken by using secondary electrons while the sample was tilted. This structure was created partly for training new SEM users but some images taken that day were also included in a science video about corrosion in space. youtu.be/GITtlkx2-Tw

 

Courtesy of Mr. Maido Merisalu , University of Tartu

 

Image Details

Instrument used: Helios NanoLab

Magnification: 3253

Voltage: 10 kV

Working Distance: 4.1 mm

Detector: SE

 

A ZnO nanostructure produced by chemical vapor deposition.

 

Courtesy of Dr. Joern Leuthold , Institute of Materials Physics, WWU Muenster

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 5000x

Horizontal Field Width: 60 µm

Vacuum: 3e-6 mbar

Voltage: 3 kV

Spot: 3

Working Distance: 5.3 mm

Detector: SE

 

The image shows an electric-transport device floating above a Silicon substrate. A thin lamella, cut from a single crystal of a heavy fermion superconductor was mircrostructured by the use of focused ion beams. It is anchored in an insulating polymer covered with Gold providing conductive paths. Our aim is to study the resistivity of exotic single-crystalline materials on the micron and sub-micron scale without any strain induced from the substrate.

 

Courtesy of Dr. Toni Helm , Max Planck Institute for Chemical Physics of Solids

 

Image Details

Instrument used: Helios NanoLab

Magnification: 2,500x

Horizontal Field Width: 160 um

Vacuum: 4e-5 mbar

Voltage: 10.0 kV

Spot: 0.17 nA

Working Distance: 4.1 mm

Detector: ETD

 

3D-Nanoprinting of a the world smallest gothic cathedral with the FEBID (Focused electron beam induced deposition) technique. The Architecture is made out of a nanogranular material (Platinum grains in carbon matrix)

 

Courtesy of Mr. Robert Winkler , Graz, centre for electron microscopy

 

Image Details

Instrument used: Other DualBeam (Altura, Expida, etc.)

Magnification: 7500x

Horizontal Field Width: 11.8µm

Vacuum: 1E-6mbar

Voltage: 2

Working Distance: 5mm

Detector: TLD

 

Electropolishing of a copper sample in H3PO4 solution did not result in the desired mirror-like surface required for EBSD.

Investigating for the problem in the SEM it turned out, that a rough surface developed because oxygen-bubbles have formed on the anode during the electro-chemical process. At locations where bubbles have covered the surface, the removal of material was reduced and, for this reason, their shapes were etched into the material.

 

Courtesy of Dr. Joern Leuthold , Institute of Materials Physics, WWU Muenster

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 1000 x

Horizontal Field Width: 300µm

Vacuum: 4e-6 mbar

Voltage: 5 kV

Spot: 3

Working Distance: 5

Detector: vCD

 

This material is a mixed lanthanum, titanium and copper oxide with perovskite structure, used as catalyst in processes of wastewater treatment.

A cross section made by a focused ion beam (FIB) shows a very porous inner structure, with a similar appearance to a sponge.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 5000x

Horizontal Field Width: 59.7 μm

Vacuum: 10e-4Pa

Voltage: 30kV

Spot: 5.5

Working Distance: 10 mm

Detector: SE

 

Surface of activated carbon used as adsorbent in water treatment processes.

Activated carbons are porous nature materials with high internal surface which gives them excellent adsorbent properties. This carbon has been prepared from biomass waste, specifically from walnut shells.

 

Courtesy of Dr. Maria Carbajo

 

Image Details

Instrument used: Quanta 3D

Magnification: 700x

Horizontal Field Width: 250 μm

Vacuum: 10-3 Pa

Voltage: 5 kV

Spot: 5.0

Working Distance: 10 mm

Detector: SE

 

boron carbide in an in-situ reactive sintering with secondary phases

 

Courtesy of Dr. Mauro Mazzocchi , Italian National Council of Research

 

Image Details

Instrument used: Quanta SEM

Magnification: 3000X

Spot: 2.7

Working Distance: 9.0

Detector: BSE

 

Abstract.

Residual stress patterns in the filter case from a polarising filter - used the filter plus another one under the subject to give the birefringence colours. True macro (approx. 2.7:1).

Sandia National Laboratories researchers Michael Chandross, left, and Nicolas Argibay show a computer simulation and an ultrahigh vacuum tribometer used in friction and wear testing, which are among the tools they use in a collaborative effort that developed a model to predict the friction behavior of metals. The goal is to understand friction and wear of materials at the most fundamental level.

 

Learn more at bit.ly/2o6QLlp.

 

Photo by Randy Montoya.

Colorized low vacuum SEM image of mold spores

 

Courtesy of Dr. Evgeny Modin , NRC Kurchatov Institute

 

Image Details

Instrument used: Versa 3D

Magnification: 8000

Horizontal Field Width: 50 um

Vacuum: 60 Pa

Voltage: 5 kV

Spot: 24 pA

Working Distance: 6.0

Detector: LVSD

 

A SEM image of a US nano flag attached on a SPM tip which can be waved. This flag is a result of skillful nano-manipulation and FIB fabrication. 50 stars and 13 strips shown on the flag were made by FIB GIS assisted Pt deposition. It paved a way en route to fabricate complex functional 3D nano-structures. Credit: J.B. Jeon, A. Klick and Moon Kim

 

Courtesy of Prof. Moon Kim , University of Texas at Dallas

 

Image Details

Instrument used: Other FEI DualBeam (Altura, Expida, etc.)

Magnification: 2500X

Voltage: 30 kV

Detector: SE

 

The provided image is a representation of structure formed by intermetallic of Si and Ni on a SiC fiber .

The fibrous structure is made by inert-pyrolysis method. The structure is used for preparing porous material being used in absorption . It is also used as catalyst.

The similarity to a "Seekh Kabab" inspired me to take an image for contest.

  

Courtesy of Mr. ARVIND KUMAR , NATIONAL INSTITUTE OF TECHNOLOGY ROURKELA INDIA

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 4,000x

Horizontal Field Width: 20 μm

Vacuum: 0.00003 mbar

Voltage: 10KV

Spot: 3.0

Working Distance: 4.6

Detector: ETD (SE)

 

A crack in magnetite superlattice film on silicon.

 

Courtesy of Mr. Zhongyue Luan , University of California, Irvine

 

Image Details

Instrument used: Magellan

Magnification: 225890

Horizontal Field Width: 917 nm

Voltage: 10 kV

Working Distance: 4.2

Detector: SE

 

The image was taken on the outer edge of a fractured tensile specimen, which was tested at elevated temperatures. The "forest" is composed of copper oxide, and the fracture surface is located on the back of the "mountain" close to the "glacier."

 

Courtesy of Dr. Joern Leuthold , Institute of Materials Physics, WWU Muenster

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 20000x

Horizontal Field Width: 15µm

Vacuum: 4e-6mbar

Voltage: 5kV - LE 2kV

Spot: 3

Working Distance: 5.3 mm

Detector: vCD

 

CVD grown ZnO micro- structures gron on n-type silicon substrate.

 

Courtesy of Prof. Abdul Majid , Majmaah University

 

Image Details

Instrument used: Quanta SEM

Magnification: 2170

Horizontal Field Width: 20

Voltage: 30

Spot: 5

Working Distance: 2.7

Detector: SE

 

pollen

 

Courtesy of Ms. Laura Schlimgen

 

Image Details

Instrument used: Other SEM (XL SEM, Sirion, etc.)

Magnification: 250x

Voltage: 25kV

Spot: 6.1

Working Distance: 11.2

Detector: BSE

 

Multiwalled carbon nanotube filled with crystalline material.

 

Courtesy of Ms. Elzbieta Pach , Institut Catala de Nanociencia i Nanotecnologia (ICN2)

 

Image Details

Instrument used: Titan

Magnification: 1.8 Mx

Horizontal Field Width: 49.7 nm

Voltage: 300 kV

 

SEM images of palladium encapsulated in silicon oxide nanotubes were taken in a high vacuum mode using a mixed signal from SE and BSE detectors.

 

Courtesy of Dr. Svetlana Neretina

 

Image Details

Instrument used: Quanta SEM

Magnification: 20,000x

Horizontal Field Width: 10.4 um

Vacuum: high vacuum

Voltage: 30 kV

Working Distance: 8.7 mm

Detector: SE and BSE

 

Catalysts of zinc oxide. Research developed by the area of Catalysis and Chemical Processes (DCAP) - INT - MCTI.

False colors are produced by mixing SE, BSE-compo and BSE-topo.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 2,293x

Horizontal Field Width: 112 µm

Voltage: 20 kV

Spot: 4.0

Working Distance: 10

Detector: Mix: SE plus BSE-compo plus BSE-topo

 

Defect made of silver paste, similar to the famous "Semeuse" engraved by Oscar Roty . This character has been widely used for french coins.

 

Courtesy of Dr. Cyril GUEDJ

 

Image Details

Instrument used: Other FIB (V600, Vectra, etc.)

Magnification: 50 X

Horizontal Field Width: 2.2 mm

Vacuum: 1mbar

Voltage: 5 kV

Spot: 1.0

Working Distance: 5.0

Detector: SE

 

Comparison of the same TEM micrograph taken in bright field and dark field.

The material is a mixed oxide of lanthanum and ruthenium with perovskite structure, used as catalyst in advanced oxidation processes.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Tecnai

Magnification: 43000x

Voltage: 200kV

Spot: 2

Detector: CCD

 

Inside of a multilayers photovoltaic panel. The cross section was perfomed with FIB.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 10000x

Horizontal Field Width: 29.8μm

Voltage: 20kV

Spot: 5.5

Working Distance: 10.5mm

Detector: SE

 

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