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ZnO has large exciton binding energy of about 60 meV so they can be used

as transparent electrodes in displays and metal oxide

semiconductor in optoelectronic devices. ZnO also is an attractive

piezoelectric materials mainly used in surface accuostic waves

components and piezoelectric devices.

 

Courtesy of Mrs. Seydanur Kaya , Kastamonu University

 

Image Details

Instrument used: Quanta SEM

Magnification: 40000x

Horizontal Field Width: 5μm

Vacuum: 3,50-e4Pa

Voltage: 20kV

Spot: 2,5

Working Distance: 10.8

Detector: SE

 

Nanoparticles of cobalt, covered by carbon deposits; catalyst after few hours of work.

 

Courtesy of Mr. Michał Rawski , Maria Curie-Sklodowska University in Lublin

 

Image Details

Instrument used: Titan

Magnification: 380000

 

The image presents a boundary between two alpha-alumina grains within an oxide scale formed on a Ni-based superalloy during high temperature oxidation at 1100 °C .

 

Courtesy of Dr. Radosław Swadźba , Institute for Ferrous Metallurgy

 

Image Details

Instrument used: Titan

Magnification: 1.4MX

Voltage: 300 kV

Spot: 3

 

Nanoplankton from the north Pacific Ocean

 

Courtesy of Mr. Marcos Rosado , Institut Catala de Nanociencia i Nanotecnologia

 

Image Details

Instrument used: Magellan

Magnification: 25000x

Voltage: 1 kV

Detector: SE + BSE

 

Synthesis of CsPbBr3 perovskite cubes are arranged side by side through out the wire like a buildings

 

Courtesy of Mr. Durga Prasad Muvva , UGC-Networking Resource Centre, School of Chemistry and The Centre for Nanotechnology, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 19.5 kx

Voltage: 200 kV

Spot: 1

Working Distance: 3

 

TEM image of Fe2O3 nanoparitcles with a flower-like shape.

 

Courtesy of Dr. Ming Lin , IMRE

 

Image Details

Instrument used: Titan

Magnification: 69,000

 

Carbon nanofiber with diamond shaped copper crystal.

 

Courtesy of Mr. Durga Prasad Muvva , UGC-Networking Resource Centre, School of Chemistry and The Centre for Nanotechnology, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 19.5 kx

Voltage: 200 kV

Spot: 1

Working Distance: 3

 

The image corresponds to a titanium, aluminum and vanadium powder alloy (Ti6Al4V).

It is the starting powder for the synthesis of biomaterials used in prosthetics and medical implants.

 

Courtesy of Dr. Maria Carbajo

 

Image Details

Instrument used: Quanta 3D

Magnification: 5000x

Horizontal Field Width: 60 μm

Vacuum: 10e-3 Pa

Voltage: 10 kV

Spot: 5.0

Working Distance: 10 mm

Detector: SE

 

ZnO microparticles obtained by hydrothermal synthesis using microwave heating.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 20,000x

Horizontal Field Width: 14.9 µm

Voltage: 20 kV

Spot: 3.0

Working Distance: 10

Detector: LFD

 

Rough cut into structured IP photoresist. Structure was written with the 3D laser lithography system Nanoscribe. The „woodpile“ was milled for an inside analysis.

  

Courtesy of Dr. Thomas Loeber , TU Kaiserslautern NSC

 

Image Details

Instrument used: Helios NanoLab

Magnification: 3,500

Horizontal Field Width: 59,2

Voltage: 2 kV

Working Distance: 3,7

Detector: SE

 

Spatial structure of the test (hard shell) of a sea urchin. Image taken by SEM FEI QEMSCAN 650F in Electron Microscopy Laboratory in PORT Polish Center for Technology Development.

 

Courtesy of Mrs. Anna Siudzinska , PORT Polish Center for Technology Development

 

Image Details

Instrument used: QEMSCAN

Voltage: 10 kV

Detector: ETD (SE)

 

Image of fabric layer of a wound dressing, which comprises of different polymers. Image was taken for characterisation purposes.

 

Courtesy of Ms. Angela Harrison , smith and nephew

 

Image Details

Instrument used: Inspect

Magnification: 482x

Horizontal Field Width: 500um

Vacuum: 50mbar

Voltage: 10kv

Spot: 3.5

Working Distance: 11.2

Detector: LFD

 

TiCN thin CVD coating deposited on a hard metal substrate was milled using a dual beam FIB-SEM to produce a micro-pillar. The surrounding textured walls are the remains of the milled bulk material, which gives an impression of the fictional city "Minas Tirith" in the film "Lord of the Rings".

 

The micro-pillar will be compressed to investigate the deformation behaviour of such tribological layers.

 

Courtesy of Mr. Idriss EL AZHARI , Chair of Functional Materials, Saarland University

 

Image Details

Instrument used: Helios NanoLab

Magnification: 17500x

Horizontal Field Width: 7.31µm

Vacuum: 0.3mbar

Voltage: 10kV

Spot: 0.34nA

Working Distance: 4.1mm

Detector: SE

 

Encapsulation

 

Courtesy of Ms. MİNE BAHCECİ

 

Image Details

Instrument used: Quanta SEM

Magnification: 9000x

Voltage: 3 kV

Spot: 3.0

Working Distance: 10.0

Detector: SE

 

Moth made of bacteria on the leaf x-cut.

 

Courtesy of Mr. Michał Rawski , Maria Curie-Sklodowska University in Lublin

 

Image Details

Instrument used: Tecnai

 

The fracture surface of a cold-rolled Pd-based glass sample. The vein patterns are clearly visible and highlighted in reddish colors. More smooth areas got a green-to-blue color depending on their respectiv brightness.

 

Courtesy of Mr. Vitalij Hieronymus-Schmidt , University of Muenster

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 7500x

Horizontal Field Width: 19.9 µm

Vacuum: 2.2e-6 mbar

Voltage: 5keV

Spot: 3.0

Working Distance: 5.1

Detector: BSE

 

The image represents a fracture into a leaf from a decorative plant. It was made using the GSED detector, in SE mode, at a 10kV, spot 4.

 

Courtesy of Dr. Berbecaru Andrei , UPB-ECOMET

 

Image Details

Instrument used: Quanta SEM

Magnification: 2,500x

Horizontal Field Width: 166

Voltage: 10kV

Spot: 4.0

Working Distance: 5.1

Detector: GSED - SE

 

This is a 3D volume reconstruction of a forest of carbon nanotubes (CNT) embedded in epoxy, visualized using Amira. The TEM sample was prepared by focusing ion beam milling in a FEI Helios FIB and imaged in a Titan TEM using TIA's tomography suite. The tilt series was reconstructed using the SIRT algorithm on Inspect 3D. The reconstruction was then processed in an in-house software to identify CNT bundles and color them based on their size. This bundling information in key to understanding the network properties as well the axial mechanical properties of these composites.

 

Courtesy of Dr. Bharath Natarajan , National Institute of Standards and Technology

 

Image Details

Instrument used: Titan

Horizontal Field Width: 896 nm

Voltage: 300 kV

Spot: 3

Detector: GIF

 

The Nano-crystalline Multi-phase Al-Pb-W alloy prepared by using ion polishing.

 

Courtesy of Mr. Durga Prasad Muvva , UGC-Networking Resource Centre, School of Chemistry and The Centre for Nanotechnology, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 7000x

Voltage: 200 kV

Spot: 1

Working Distance: 3

 

Replica of the glass pyramids in the courtyard of the Louvre (Paris) in a scale of 1: 8.000.000. The basement and the fountains are a FIB-cut, the 3D-structures (branch sizes between 25 and 70 nm) consist of platinum and carbon and were fabricated in a consecutive process step in the same instrument (FEI FIB Nova). This image demonstrates the 3D-Nanoprinting capabilities of Focused Electron Beam Induced Deposition (FEBID). Compare it to the real Louvre!

  

Courtesy of Mr. Robert Winkler , Graz, centre for electron microscopy

 

Image Details

Instrument used: Other FEI DualBeam (Altura, Expida, etc.)

Magnification: 5000x

Horizontal Field Width: 19.5 µm

Vacuum: 5E-6mbar

Voltage: 30 kV

Working Distance: 5 mm

Detector: SE, ETD

 

TheraCal is a new light-curable dental material composed of calcium silicate and resin, for use as a pulp-capping material and liner, in restorative dentistry. The image shows a calcium silicate crystal seen in a sample from a study to evaluate the apatite forming ability of TheraCal, which is critical for new dentin formation.

 

Courtesy of Dr. Ravi Sidhu , University of Manitoba

 

Image Details

Instrument used: Quanta SEM

Magnification: 17,993x

Horizontal Field Width: 11.5 um

Vacuum: 6.72e-4 Pa

Voltage: 10kV

Spot: 3.5

Working Distance: 10.7

Detector: BSE

 

This breathtaking flower-like structure actually marks the end of a polymer-aluminium oxide nanocomposite coating as it is the first sign of corrosion. The coating wasn't developed further as the "blooms of death" always came back and ultimately the whole coating failed already within 7 days. For taking the image, the sample was tilted and secondary electrons were used.

 

Courtesy of Mr. Maido Merisalu , University of Tartu

 

Image Details

Instrument used: Helios NanoLab

Magnification: 1500

Detector: SE

 

Biochar is a highly porous carbon-rich material produced by pyrolysis of biomass. The SEM image shows micropores in a wood-derived biochar sample. Due to its unique properties such as high porosity, large surface area, and presence of negatively charged organic functional groups, biochar is used as adsorbent for the removal of various contaminants in soil and wastewater. Biochar is a simple yet powerful tool for soil and waste management, energy production, and C-sequestration to mitigate climate change.

 

Courtesy of Dr. Ravi Sidhu , University of Manitoba

 

Image Details

Instrument used: Quanta SEM

Magnification: 4000x

Horizontal Field Width: 5

Vacuum: 100 Pa

Voltage: 10kV

Spot: 3.0

Working Distance: 9.3

Detector: LFD

 

The silicon nanopillars are fabricated through combining two techniques, a gold mask made by nanosphere lithography and a Metal-Assisted Chemical Etching of Silicon.

The structures shown in the image look like the Amazon River, but at the nanoscale.

  

Courtesy of Marcos Rosado

 

Image Details

Instrument used: Magellan

Magnification: 5000x

Horizontal Field Width: 59.7 um

Vacuum: 5 x 10E-5 Pa

Voltage: 2kV

Spot: 100 pA

Working Distance: 5.6

Detector: vCD

 

Transmission electron microscope of mosquito skin surface showing air follicles.

 

Courtesy of Mr. Durga Prasad Muvva , Iconanalytical Equipments, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 1k

Horizontal Field Width: 2.00um

Voltage: 200 V

Spot: 3

Working Distance: 3

 

Alginic acid is a heteropolysaccharide composed of D-mannuronic and L-guluronic acids. In nature it can be obtained from organisms as diverse as brown seaweed and bacteria. It is non-toxic, has a high molecular weight and a high viscosity. Due to its physico-chemical characteristics, it has been widely used as a phase stabilizer in food and beverages, as well as in the pharmaceutical industry. Another very important area of application is environmental protection: alginate gels are used as adsorbents for the removal of heavy metals such as cadmium, zinc, lead, chromium and mercury from wastewater. In the micrograph, Zinc crystals are observed that have been adsorbed on the surface of an alginate gel after being subjected to a process of wastewater treatment.

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 8000x

Horizontal Field Width: 37μm

Voltage: 15kV

Spot: 5.0

Working Distance: 10mm

Detector: SE

 

Detail of the dentinal tubules viewed after demineralization process.

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 13,462

Horizontal Field Width: 11 µm

Vacuum: 130 Pa - Low Vacuum

Voltage: 10 kV

Working Distance: 11.1

Detector: MIX: SE plus BSE

 

Aerators should be regularly kept cleaned or replaced.

The mesh in the aerator can collect lead debris, and then leach this toxic metal into the water passing through it.

Aerators cap the ends of most drinking-water faucets. In some cases, they’re used to conserve water by reducing a faucet’s maximum flow rate; in others their primary function is to concentrate the flow of water so that it delivers more pressure and cleaning power. But these little metal cages also collect debris. Including lead. And unless you’re regularly cleaning out those aerators, you might be developing a toxic mini gravel field through which your drinking water must pass before reaching your glass or coffee pot.

Indeed, one lead poisoning case in North Carolina involved a child (see link below):

www.dcwater.com/waterquality/faqs.cfm

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 70x

Horizontal Field Width: 4.26 mm

Vacuum: 90 Pa

Voltage: 20 kV

Spot: 4.0

Working Distance: 15.6

Detector: Mix: SE plus BSE

 

ZnO micro-flowers obtained by hydrothermal synthesis using microwave heating.

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 15,000X

Horizontal Field Width: 19.9 μm

Vacuum: 80 Pa

Voltage: 20 kV

Spot: 3.0

Working Distance: 10

Detector: MIX: SE plus BSE

 

The image presents an aglomeration of iron oxides nanostructures obtained by laboratory synthesis. The image was made in HV, at 30kV, spot 3.0.

 

Courtesy of Dr. Berbecaru Andrei , UPB-ECOMET

 

Image Details

Instrument used: Quanta SEM

Magnification: 160,000x

Horizontal Field Width: 2.59

Vacuum: High Vacum

Voltage: 30

Spot: 3.0

Working Distance: 5.8

Detector: SE

 

The cubic nanoparticles are 13 nm-sized iron oxide crystals. They were synthesized by a colloidal chemistry route and deposited on a TEM grid, tending to self-assembling. The lighter zones around the nanocubes assemblies are made of organic residuals left on the thin carbon film substrate. This image was taken with no tilt and everything was false-colored.

 

Courtesy of Prof. Andrea Falqui , King Abdullah University of Science and Technology (KAUST)

 

Image Details

Instrument used: Magellan

Magnification: 75000

Horizontal Field Width: 1.8 µm

Vacuum: High Vacuum

Voltage: 5 kV

Spot: 3.0

Working Distance: 2.9

Detector: TLD

 

Platinum can be deposited with electron beam lithography and a gas injection system. We also use a pattern generator to create and structure large areas. Here we patterned the Koch snowflake, which is designed by using only triangles in different sizes. Starting with a first large equilateral triangle then three triangles with only one third of its length are attached in the middle of each side of the first one. This was repeated several times. For demonstration the Christmas card was done with this procedure to show our users the capability of the system.

 

Courtesy of Dr. Thomas Loeber , TU Kaiserslautern NSC

 

Image Details

Instrument used: Helios NanoLab

Magnification: 4496

Horizontal Field Width: 46.1

Voltage: 5

Working Distance: 3.9

Detector: TLD

 

Aerators should be regularly kept cleaned or replaced.

The mesh in the aerator can collect lead debris, and then leach this toxic metal into the water passing through it.

Aerators cap the ends of most drinking-water faucets. In some cases, they’re used to conserve water by reducing a faucet’s maximum flow rate; in others their primary function is to concentrate the flow of water so that it delivers more pressure and cleaning power. But these little metal cages also collect debris. Including lead. And unless you’re regularly cleaning out those aerators, you might be developing a toxic mini gravel field through which your drinking water must pass before reaching your glass or coffee pot.

Indeed, one lead poisoning case in North Carolina involved a child (see link below):

www.dcwater.com/waterquality/faqs.cfm

  

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 127x

Horizontal Field Width: 2.34 mm

Vacuum: 90 Pa

Voltage: 20 kV

Spot: 3.0

Working Distance: 14.7

Detector: Mix: SE plus BSE

 

Pt nanoparticles embed in alumina, used for chemisorption measurements.

 

Courtesy of Mr. Michał Rawski , Maria Curie-Sklodowska University in Lublin

 

Image Details

Instrument used: Titan

 

It's an environmental scanning electron microscope image of the fracture surface of an effervescent tablet of Vitamin C.

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 1,500x

Horizontal Field Width: 199 μm

Vacuum: 300 Pa

Voltage: 10 kV

Spot: 3.0

Working Distance: 12.9

Detector: MIX: GAD plus LFD

 

Nanoparticles of titanium dioxide used as a catalyst in processes of photocatalysis.

  

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Tecnai

Magnification: 80000x

Voltage: 200kV

Detector: CCD

 

Biocarbon used for water filtration.

 

Courtesy of Mr. Michał Rawski , Maria Curie-Sklodowska University in Lublin

 

Image Details

Instrument used: Quanta 3D

Magnification: 350x

Horizontal Field Width: 426μm

Voltage: 20kV

Working Distance: 10

Detector: ETD

 

Inside view of a semiconductor integrated circuit (IC) chip with micro-structure-surface passivation film.

The cross-section was performed using focused ion beam (FIB).

 

Courtesy of Dr. Maria Carbajo , UNIVERSIDAD DE EXTREMADURA

 

Image Details

Instrument used: Quanta 3D

Magnification: 16000

Horizontal Field Width: 18 μm

Vacuum: 10e-4 Pa

Voltage: 10 kV

Spot: 6.0

Working Distance: 10.7 mm

Detector: SE

 

This is image of the Ti35Nb alloy. Titanium alloys form the most versatile group of metallic materials used as biomaterials. Its alloys are frequently utilized as implant materials in dentistry and orthopedic surgery.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 8,000x

Horizontal Field Width: 37.3 µm

Voltage: 20 kV

Spot: 4.5

Working Distance: 16.3

Detector: Mix: SE plus BSE.

 

Catalysts of zinc oxide. Research developed by the area of Catalysis and Chemical Processes (DCAP) - INT - MCTIC.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 2,293x

Horizontal Field Width: 130 µm

Voltage: 20 kV

Spot: 4.0

Working Distance: 10

Detector: Mix: SE plus BSE

 

Pollen grain extracted from a forensic soil sample and observed in ESEM mode. It is possible to clearly see the features of Its sculpture and Its apertural system.

 

Courtesy of Mr. Francisco Torres

 

Image Details

Instrument used: Quanta 3D

Horizontal Field Width: 32 um

Vacuum: 701 Pa

Voltage: 15 kV

Spot: 5

Working Distance: 6.5 mm

Detector: GSED

 

This scanning electron microscopy image shows a small portion of the surface of a garden wooden table. Non-expected crystalline features appeared on the SEM image when analyzing the sample. Amorphous-like content can be seen in false yellow/brown color and crystalline structures are shown in blue/purple false colors. There is no scientific significance in the image shown but the beauty of the micro/nano world can also be admired in non-scientific purpose images like this one. The sample was imaged on the Magellan 400L XHRSEM, no conductive coating applied to the sample.

 

Courtesy of Mr. Marcos Rosado , Institut Catala de Nanociencia i Nanotecnologia

 

Image Details

Instrument used: Magellan

Magnification: 10000x

Horizontal Field Width: 30 um

Vacuum: High vacuum

Voltage: 2 kV

Spot: 100 pA

Working Distance: 5 mm

Detector: BSE beam deceleration

 

This is image of the Ti35Nb alloy. Titanium alloys form the most versatile group of metallic materials used as biomaterials. Titanium and Its alloys are frequently utilized as implant materials in dentistry and orthopedic surgery.

 

Courtesy of Mr. FRANCISCO RANGEL , MCTI/INT

 

Image Details

Instrument used: Quanta SEM

Magnification: 6,000x

Horizontal Field Width: 49.7

Voltage: 20 kV

Spot: 4.5

Working Distance: 14.9

Detector: Mix: SE plus BSE.

 

Department of Materials Science and Metallurgy, Cambridge

Zinc Nano Oxide Flower formed by Zinc Nitrate and Hexamethylenetetramine (HMT) as a precursors on Silicon substance for a period of 10 Hrs. at 90 degree Celsius.

The work involves the fabrication of nano structures exploited to create GAS SENSOR .

Zinc nitrate and Hexamethylenetetramine (HMT) is a useful chemical component for testing molecular Gas sensor with a well known chemistry with important Industrial application(from Hazard Gases).

The amazing similarity to a real Flower inspired me to take an image for contest.

  

Courtesy of Mr. SHIV KUMAR VERMA , NIT ROURKELA

 

Image Details

Instrument used: Nova NanoSEM

Magnification: 18,755X

Horizontal Field Width: 4μm

Vacuum: 0.00003mbar

Voltage: 10KV

Spot: 3.0

Working Distance: 4.4

Detector: SE

 

Nanoplankton from the north Pacific Ocean.

 

Courtesy of Mr. Marcos Rosado , Institut Catala de Nanociencia i Nanotecnologia

 

Image Details

Instrument used: Magellan

Magnification: 15000x

Voltage: 1 kV

Detector: SE + BSE

 

Cross-transverse view of a cigarette filter, showing cellulose acetate fibers.

Ingestion or inhalation of fragments of cigarette filter fibers is a health problem for almost all smokers, but also contributes to the formation of lung cancer.

Smoking is a trap. Quit now!

 

Courtesy of Mr. FRANCISCO RANGEL

 

Image Details

Instrument used: Quanta SEM

Magnification: 2500x

Horizontal Field Width: 119 µm

Vacuum: 110 Pa

Voltage: 20 kV

Spot: 3.0

Working Distance: 15.1

Detector: MIX: SE plus BSE

 

Carbon fiber or carbon fibre (alternatively CF, graphite fiber or graphite fibre) is a material consisting of fibers about 5–10 micrometres in diameter and composed mostly of carbon atoms.

 

To produce carbon fiber, the carbon atoms are bonded together in crystals that are more or less aligned parallel to the long axis of the fiber as the crystal alignment gives the fiber high strength-to-volume ratio (making it strong for its size). Several thousand carbon fibers are bundled together to form a tow, which may be used by itself or woven into a fabric.

 

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MORE INFORMATION

 

Images in this gallery were captured by:

 

Mark Smith M.S. Geoscientist mark@macroscopicsolutions.com

 

Annette Evans Ph.D. Student at the University of Connecticut annette@macroscopicsolutions.com

It is an aberration corrected TEM image acquired from a multi-walled carbon nanotube filled with iron nanowire. This image is acquired by Dr. Mert Kurttepeli and Dr. Nadja Tarakina with an FEI Titan microscope operated at 120 kV equipped with an image correcter, a probe correcter and a monochromator. The image itself enables us to understand the interaction between the iron nanowire with the carbon nanotube and to see if there is any direct link between those two.

 

Courtesy of Dr. Mert Kurttepeli , Electron Microscopy for Materials Science (EMAT)-University of Antwerp

 

Image Details

Instrument used: Titan

Magnification: 295,000x

Horizontal Field Width: 13.66nm

Voltage: 120 kV

Spot: 2.0

 

Green synthesis of Au Triangles by false color

 

Courtesy of Mr. Durga Prasad Muvva , UGC-Networking Resource Centre, School of Chemistry and The Centre for Nanotechnology, University of Hyderabad

 

Image Details

Instrument used: Tecnai

Magnification: 71000x

Voltage: 200 kV

Spot: 1

Working Distance: 3

 

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