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Micro-molded part from a deep-etched silicon mold.
Bad adhesion of metallization.
Titanium oxide crystallite during the deposition of a wet-chemical layer
Plasma etching done by SF6 plasma in the so-called Bosch process.
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DoITPoMS, University of Cambridge
Using this alloy composition, a relatively low volume fraction of pro-eutectic dendrites is formed. Due to their different chemistry the eutectic interdendritic Sm and Cu enriched phases material between these dendrites can be etched away to reveal the three-dimensional structure of dendrites. The dendrite tips are a volume have the form of a paraboloid of revolution, and anisotropy develops behind them with the secondary dendrite arms.
See R. Glardon, W. Kurz, "Solidification path and phase diagram of directionally solidified Co-Sm-Cu alloys", J. Cryst. Growth, 51 (1981) 283-291.
System
Co-Sm-Cu
Composition
Co 70, Sm 10, Cu 20 (at%)
Reaction
Processing
Directionally solidified in a Bridgman apparatus
Applications
Sample preparation
After directional solidification the cobalt-samarium-copper alloy has been deeply etched with 10% nitric acid in ethyl alcohol (10%Nital) to remove the eutectic material Sm and Cu enriched phases between the primary dendrites.
Technique
Scanning electron microscopy (SEM)
Contributor
Prof W Kurz
Organisation
Department of Materials, Swiss Federal Institute of technology (EPFL), Lausanne, Switzerland
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